Analyses of mixed sulphides containing varying small amotmts of roelm. Except in the ease~of lead all the spectral values are single determinations. The lead values are the mean of two runs. Analytical lines: Cu 5218, Zn 3345, Pb 4057 ; internal standard line: Cd 4800. ~o Cu ~o Zn ~o Pb ~ample Spect.
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The BER sample contained a variety of notable metal impurities/enrichments (Al, Fe, Ca, Cu, Zn, Pb, and Mn). The amount of metal impurities varied greatly among the remaining struvite products, e.g. Fe concentration in BER (2993 mg kg −1 ) and HER (1349 mg kg −1 ) which were substantially higher than the other struvite products (which .
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131 Dupont & Co.) in an agate planetary ball mill for half an hour. The mixture was then 132 pressed using a 25 tonne load into pellets with a thickness of 40 mm. The coeﬃcients 133 of variation for a soil sample standard were: Ni (0.6 %) Cu ( 1%) and Zn (0.8 %). 134 Soil pH and SOC were only determined on a subset of 114 sites (a total of .
Ni, Cu, Zn, As, Mo, Pb, and U in another. The elements determined and the lower limits of detection (LLD) and upper and lower reporting limits (URL and LLR) for each analy te are shown in Table 3.
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